Ambiguity
Numerical analysis shows that
one pattern is not sufficient for determination of a complete strain
tensor because the optimization problem is ill–conditioned:
adding
d3 | 0 | d1 |
0 | d3 | d2 |
d1 | d2 | a d3 |
to a strain tensor given in the
microscope coordinate system with the ’3’ along optical
axis
of the microscope has an undetectable effect on the simulated pattern; di
are
arbitrary numbers with magnitude of the order of 1/1000 and a is of the
order of 2. In order to alleviate the problem, multiple patterns with
different orientation but originating from the same area of the foil
can be used. In the case of two diffraction patterns, a unique strain
tensor can be obtained if the characteristics a are sufficiently
different. If more than two zone axes are used, the solution is, in
principle, unique. In practice, the reliability of the results may be
still low due to errors in the locations of HOLZ lines.
TEMStrain v.1.3, Dec. 2014